* Laboratory reports for these experiments are due
on the period following the completion of the experiment (completion
is noted by an asterisk). Note The extraction experiment
is three periods long, combined with recrystallization and melting
points. The dehydration of 2-methylcyclohexanol and gas chromatography
labs are combined. Late reports will only be accepted with prior
permission from the instructor.
Ý For synthesis experiments, the "Balanced
Reaction" and "Table of Reactants and Products"
must be completed before you start the lab.
| WEEK |
DATES |
LABORATORY EXERCISE |
PAGE |
| 1 |
6/2 |
Check-in and Laboratory Safety |
|
|
6/2 |
Structure and Isomerism (worksheet) |
3 |
| 2 |
6/7 |
Molecular Conformations (worksheet) |
8 |
|
6/9 |
Thin Layer Chromatography (Technique Experiment)* |
14 |
|
6/10 |
Extraction Separation of a Mixture of Benzoic Acid
and p-Dimethoxybenzene (Technique Experiment) (note: this experiment
lasts for 3 periods) |
17 |
| 3 |
6/14 |
Recrystallization Purification of Benzoic Acid and
p-Dimethoxybenzene (Technique Experiment) |
20 |
|
6/16 |
Analysis of Extraction and Recrystallization Products |
|
|
|
by Melting Points and TLC (Technique Experiment)* |
21 |
|
6/17 |
(+)-Limonene from Orange Peel (Technique Experiment)* |
23 |
| 4 |
6/21 |
Dehydration of 2-Methylcyclohexanol (Synthesis Experiment)Ý |
|
|
6/23 |
- Gas Chromatography of Dehydration Products*
- AND Soap Making (No Report)
|
29 |
|
6/24 |
Bromination of Acetanilide (Synthesis Experiment)Ý* |
25 |
| 5 |
6/28 |
Synthesis of Ethyl Heptanoate (Synthesis Experiment)Ý |
32 |
|
6/30 |
- Qualitative Organic Unknown*
- AND Boiling Point of Ethyl Heptanoate*
|
|
|
7/1 |
Check Out |
|
Lecture Notes